Table 1.
Crystallographic Data and Refinement Statistics
| X-Ray Source | APS SER-CAT 22ID | |
|---|---|---|
| PDB ID | 3HVM | |
| Wavelength (Å) | 1.00000 | |
| Space group | P3221 | |
| Unit cell dimensions: | a (Å) | 52.08 |
| c (Å) | 246.40 | |
| Resolution Range (Å) (highest shell) | 50.0-2.10 (2.18-2.10) | |
| Mosaicity (degree) | 0.47 | |
| Completeness (%),(highest shell) | 76.0(59.8) | |
| Total linear R-merge | 0.043 | |
| Reflections Observed | 65011 | |
| I over average sigma(I) | 16.5 | |
| Redundancy, (highest shell) | 3.6 (3.2) | |
| Rmsd bonds (Å) | 0.016 | |
| Rmsd angles (°) | 1.73 | |
| Ramachandran Statistics | ||
| Residues in most favored regions (%) | 265 (88.6) | |
| Residues in additionally allowed regions (%) | 32 (10.7) | |
| Residues in generaously allowed regions (%) | 1 (0.3) | |
| Residues in disallowed regions (%) | 1 (0.3) | |
| R Refmac5 | 0.200 | |
| Rfree Refmac5 | 0.259 | |