. Author manuscript; available in PMC: 2010 Dec 1.

Published in final edited form as: Bioorg Med Chem. 2009 Oct 30;17(23):7949–7957. doi: 10.1016/j.bmc.2009.10.019

Table 6.

¹³C NMR data for 5 and 6–18 (δ_C in ppm)

Position	5^a	6^a	7^a	8^a	9^a	10^a	11^a	12^a	13^a	14^b	15^a	16^b	17^a	18^a
1/1′	52.9	52.6	52.8	52.7	52.8	52.7/52.8	52.7	52.65/52.71	52.7/52.8	53.00/53.03	52.4	53.0	52.6	52.8
2/2′	25.0	24.4/24.5/24.67/24.71	24.7/24.9	24.6/24.8	24.5/24.7/24.9	24.69/24.85/24.87	24.8	24.8/24.9	24.7/24.9	25.1/25.3	24.4/24.6	25.11/25.38	24.6/24.8	24.6/24.7/24.8/24.90/24.91
3/3′	36.9	36.4/36.5	36.6	36.6	36.62/36.64	36.59/36.63	36.6	36.6	36.6	37.1	36.3	37.1	36.5	36.7
4/4′	104.5	104.2/104.3	104.4	104.2	104.3	104.27/104.32	104.4	104.3/104.5	104.3/104.4	104.0	104.3	104.5	104.5	104.17/104.27/104.30
5/5′	88.3	88.1/88.3	88.5	88.1	88.27/88.30	88.07/88.12	88.1/88.2	88.3/88.2	88.1/88.2	88.5/88.6	88.1	88.5	88.1	88.11/88.15/88.17
6/6′	81.4	81.0/81.2	81.3	81.3	81.3/81.4	81.1/81.2	81.1/81.2	81.2	81.3	80.2/81.4	80.9	81.5	81.3	81.2/81.3
7/7′	44.8	44.42/44.44	44.7	44.6	44.59/44.64	44.5/44.6	44.4/44.5	44.5	44.55/44.56	44.9/45.0	44.1	45.1	44.5	44.64/44.69/44.74
8/8′	25.0	24.4/24.5/24.67/24.71	24.7/24.9	24.6/24.8	24.5/24.7/24.9	24.69/24.85/24.87	24.8	24.8/24.9	24.7/24.9	25.1/25.3	24.4/24.6	25.11/25.38	24.6/24.8	24.6/24.7/24.8/24.87/24.91
9/9′	35.0	34.66/34.69	34.9	34.8	34.9	33.9/34.2	34.8	34.8	34.8	35.1	34.5	35.0	34.7	34.8/34.9
10/10′	37.8	37.41/37.46	37.6	37.5	37.56/37.64	37.66/37.67	37.7	37.6/37.7	37.6/37.7	37.5/37.7	37.5	37.6	37.6	37.65/37.69
11/11′	31.3	31.0	31.3	31.0	30.9/31.2	31.1	31.1	31.0/31.4	31.0/31.1	31.56/31.64	30.7	31.7	31.0	31.1/31.2/31.6
12/12′	103.2/103.1	100.6/101.4	100.6/103.8	101.7	98.9/103.0	102.4/102.6	102.8/103.0	103.2/103.3	102.4/103.0	102.5/103.2	102.7	101.7	101.6	102.3/102.6/103.1
13/13′	13.5	13.0/13.2	13.2	13.2	13.2/13.3	13.19/13.21	13.3	13.2/13.5	13.2	13.39/13.45	13.0	13.6	13.14	13.2/13.4/13.7
14/14′	20.8	20.36/20.39	20.6	20.6	20.58/20.62	20.50/20.53	20.6	20.5/20.6	20.5	20.77/20.81	20.3	20.7	20.54	20.49/20.53
15/15′	26.5	26.0/26.2	26.3	26.3	26.4	26.29/26.34	26.3	26.4	26.3	26.3/26.5	26.0	26.5	26.2	26.4
16	70.2	69.4	158.9	64.1	71.8	73.3	70.6	63.7	67.1	67.3/67.8	71.5	70.4	58.3	71.7
17	70.1	141.2	103.8	129.2	76.4	68.7	71.4	78.5	54.4	80.2	207.8	142.0	132.7	75.6
18	70.3	108.0/108.2	148.0	129.2	135.9	33.9	71.4	71.6	55.1	67.3/67.8	66.7	106.6	128.0	33.0
19	-	156.9/158.5	109.2	64.1	119.3	65.7	70.2	69.5	66.5	-	-	160.8	63.6	64.6
20	-	103.3	130.0	-	-	-	-	-	-	-	-	103.4	-	-
21	-	156.9/158.5	107.2	-	-	-	-	-	-	-	-	160.8	-	-
22	-	108.0/108.2	-	-	-	-	-	-	-	-	-	106.6	-	-

CDCl₃.

pyridine-d₅.