Table 4.
1H shifts (ppm) | |δaxial − δequatorial | | Coalescence | ΔG | |
---|---|---|---|---|
CH2 near N(t) | 2.84 & 2.33 | 304.6 Hz | 238.6K | 10.69 kcal mol−1 |
CH2 near N(s) | 3.33 & 2.98 | 206.2 Hz | 236.5K | 10.85 kcal mol−1 |
NH2 | 9.31 & 9.62 | 187.5 Hz | 213.5K | 9.79 kcal mol−1 |
1H shifts (ppm) | |δaxial − δequatorial | | Coalescence | ΔG | |
---|---|---|---|---|
CH2 near N(t) | 2.84 & 2.33 | 304.6 Hz | 238.6K | 10.69 kcal mol−1 |
CH2 near N(s) | 3.33 & 2.98 | 206.2 Hz | 236.5K | 10.85 kcal mol−1 |
NH2 | 9.31 & 9.62 | 187.5 Hz | 213.5K | 9.79 kcal mol−1 |