Table 1. Summary of data-collection and refinement statistics for HIP1 369–445.
Data collection | |
Space group | P212121 |
Unit-cell parameters (Å, °) | a = 35.7, b = 57.0, c = 81.1, α = β = γ = 90 |
Resolution (Å) | 50–2.30 (2.38–2.30) |
Rmerge | 0.03 (0.17) |
〈I/σ(I)〉 | 32.7 (6.32) |
Completeness (%) | 99.2 (96.8) |
Redundancy | 3.9 (3.4) |
Refinement | |
Resolution (Å) | 40.6–2.30 |
No. of reflections | 7331 |
Rwork/Rfree (%) | 23/28 |
No. of atoms | |
Protein | 1281 |
Water | 39 |
B factor (mean) (Å2) | 50.3 |
R.m.s deviations | |
Bond lengths (Å) | 0.01 |
Bond angles (°) | 1.36 |