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Electrophoretic analysis of heated mixtures: (Rh[16aneS4-diol]*I) contained Rh(III) cations, 16aneS4-diol ligand, and *I−; blank 1 contained Rh(III) and *I− without sulfur ligand; blank 2 contained sulfur ligand and *I− without metal cations. Paper electrophoresis was performed on glass fiber Whatman Paper Chromedia GF83 using phosphate buffer (pH 4.0 or 7.4) at 10 V/cm for 25 min.
