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. Author manuscript; available in PMC: 2010 Mar 2.
Published in final edited form as: Bioconjug Chem. 2008 Mar 14;19(4):958–965. doi: 10.1021/bc700413r

Table 2.

Effect of 16aneS4-diol Concentration on the M[16aneS4-diol]X (M =Rh(III) or Ir(III) and X = *I or 211At) Complexes Yield at pH of ~4.0

yield ± SD [%]
quantity of
ligand nS4 (nmol)		 Rh[16aneS4-
diol]*I		 Ir[16aneS4-
diol]*I		 Rh[16aneS4-
diol]211At		 Ir[16aneS4-
diol]211At
18.75 2.1 ± 1.3 2.4 ± 1.8 3.1 ± 2.2 3.5 ± 2.6
25.0 7.4 ± 2.8 18.2 ± 1.3 9.5 ± 0.8 8.6 ± 4.5
62.5 43.8 ± 7.1 38.4 ± 1.3 48.7 ± 5.7 26.4 ± 7.6
125.0 73.8 ± 6.9 70.5 ± 3.1 69.6 ± 6.4 65.2 ± 8.7
187.5 79.4 ± 2.0 77.6 ± 2.8 76.5 ± 3.3 71.3 ± 6.5
250.0 82.1 ± 3.2 80.2 ± 2.5 78.3 ± 4.2 74.5 ± 2.8