Table 1. Data-collection statistics.
Values in parentheses are for the last resolution shell.
| Synchrotron | PLS, beamline 6B |
| Wavelength (Å) | 1.00 |
| Resolution range (Å) | 50.0–2.60 (2.64–2.60) |
| Space group | P212121 |
| Unit-cell parameters (Å) | |
| a | 98.98 |
| b | 101.56 |
| c | 141.83 |
| No. of unique reflections | 43499 |
| Redundancy | 4.7 (5.0) |
| Completeness (%) | 98.5 (99.7) |
| Molecules per asymmetric unit | 2 |
| VM (Å3 Da−1) | 3.18 |
| Solvent content (%) | 59.9 |
| Average I/σ(I) | 28.1 (3.7) |
| Rmerge† (%) | 7.8 (42.9) |
R
merge =
, where I
i(hkl) is the intensity of an individual reflection hkl and 〈I(hkl)〉 is the average intensity of reflection hkl.