. Author manuscript; available in PMC: 2011 Apr 6.

Published in final edited form as: J Pharm Biomed Anal. 2009 Nov 26;51(5):1120–1127. doi: 10.1016/j.jpba.2009.11.020

Table 1.

Compound dependent parameters for matrine and other compounds in MRM mode for UPLC–MS/MS analysis.

Analyte	Q1 mass (U)	Q3 mass (U)	Dwell time (ms)	DP (V)	CEP (V)	CE (V)	CXP (V)
Matrine	249	148	100	96	23	49	2
Testosterone	289	97	100	60	20	33	2
Rutin	611	303	100	30	37	28	4
6β-hydroxytestosterone	305	269	100	39	26	18	4
Genistein	269	133	100	−80	−22	−40	−3
Genistein 7-O-glucuronide	445	269	100	−30	−34	−40	−3
Rutin	609	300	100	−50	−31	−49	−2