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Analysis of the products from reactions of apo-Fbp with [Cp2Nb(OH)Cl2] and [Nb(NTA)2]−.
| Reaction mixture(a) | Product(b) | Reaction mixture | Product |
|---|---|---|---|
| [Cp2Nb(OH)Cl2]/[Fbp] | [Nb]/[Fbp] | [Nb(NTA)2]−/[Fbp] | [Nb]/[Fbp] |
| 1 : 1 | 0.86 ± 0.10 : 1 | 1 : 1 | 0.91 ± 0.10 : 1 |
| 20 : 1 | 2.23 ± 0.10 : 1 | 20 : 1 | 2.41 ± 0.10 : 1 |
(a) Reactions carried out for 48 hours in 10 mM HEPES buffer, pH 7.4, 310 K.
(a)Fbp concentration determined from A280.
