UV/Vis spectra of aqueous solutions of 9 (initial concentration = 25.5 μM) after exposure to an equal volume of a CH2Cl2 solution of polymer 4 (effective concentration of the calix[4]pyrrole and crown ether repeat units was 1.56 and 1.22 mM, respectively), 1 (1.56 mM), 3 (1.22 mM), or a mixture of 1 and 3 (1.56 and 1.22 mM, respectively).