Table 1. Crystal information and data-collection statistics.
Values in parentheses are for the outer resolution shell.
| Beamline | SPring-8, BL41XU |
| Detector | ADSC Quantum 315 |
| Wavelength (Å) | 1.00 |
| Beam size (µm) | 100 |
| Temperature (K) | 100 |
| Space group | P3121 or P3221 |
| Unit-cell parameters (Å) | a = b = 111.3, c = 192.4 |
| Resolution (Å) | 50.0–2.5 (2.58–2.5) |
| No. of reflections (total/unique) | 454742/48923 |
| Completeness (>0σ) (%) | 92.6 (44.3) |
| Mosaicity | 0.906 |
| 〈I/σ(I)〉 | 18.1 (0.73) |
| Rmerge† (%) | 9.1 (35.2) |
| Average redundancy | 9.3 (8.3) |
†
R
merge = 
, where I
i(hkl) is the ith observation of reflection hkl and 〈I(hkl)〉 is the weighted average intensity for all observations i of reflection hkl.