Table 1. Data-collection statistics for PfADF1 and PbADF2.
Values in parentheses are for the highest resolution shell.
| PfADF1 | PbADF2 | |
|---|---|---|
| Beamline | I911-2 | I911-3 |
| Wavelength (Å) | 1.0380 | 0.9790 |
| Beam size (mm) | 0.3 × 0.3 | 0.15 × 0.25 |
| Space group | P3121/P3221 | P21212 |
| Crystal dimensions (mm) | 0.2 × 0.15 × 0.15 | 0.2 × 0.05 × 0.05 |
| Unit-cell parameters | a = b = 68.84, c = 76.03, α = β = 90, γ = 120 | a = 111.58, b = 57.90, c = 40.49, α = β = γ = 90 |
| Resolution range (Å) | 20.0–2.0 (2.05–2.0) | 20–2.1 (2.15–2.1) |
| Oscillation per frame (°) | 1 | 0.25 |
| No. of frames collected | 180 | 653 |
| No. of measured reflections | 145966 (7050) | 97420 (7461) |
| No. of unique reflections | 14010 (1004) | 15859 (1168) |
| Criterion for observed reflections [I/σ(I)] | −3 | −3 |
| Multiplicity | 10.4 (7.0) | 6.1 (6.4) |
| Completeness (%) | 96.5 (94.5) | 99.1 (99.8) |
| Average I/σ(I) | 38.5 (14.5) | 16.4 (4.2) |
| Rmerge† (%) | 4.6 (27.5) | 6.0 (64.9) |
†
R
merge = 
, where I
i(hkl) is the intensity of the ith measurement of reflection hkl and 〈I(hkl)〉 is the mean intensity of reflection hkl.