| Resolution (Å) |
18–0.90 |
15–0.95 |
| No. of reflections, working set |
163837 |
147440 |
| No. of reflections with Fo > 4σ(Fo), working set |
123349 |
115415 |
| No. of reflections, test set |
8614 |
7313 |
| No. of reflections with Fo > 4σ(Fo), test set |
6462 |
6041 |
|
Rcryst, Fo > 4σ(Fo) |
0.125 |
0.109 |
|
Rcryst, all data |
0.141 |
0.119 |
|
Rfree, Fo > 4σ(Fo) |
0.143 |
0.130 |
|
Rfree, all data |
0.160 |
0.141 |
| R.m.s. deviation from ideal bond lengths (Å) |
0.033 |
0.030 |
| No. of protein atoms |
2098 |
2120 |
| No. of heteroatoms |
22 |
58 |
| No. of solvent atoms |
364 |
338 |
| Residues in (%) |
88.9 |
88.5 |
| Most favored regions (%) |
88.9 |
88.5 |
| Additional allowed regions (%) |
11.1 |
11.0 |
| Generously allowed and disallowed regions (%) |
0.0 |
0.5 |
