Table III.
Data Collection and Refinement Statistics
| PDLIM1 | PDLIM2 | PDLIM4 | PDLIM5 | PDLIM7 | GRASP | MAST4 | |
|---|---|---|---|---|---|---|---|
| Crystal form | |||||||
| Unit Cell [a, b, c (Å), β/γ (°)] | 38.7, 38.7, 246.5 | 58.8, 58.8, 52.3 | 87.0, 87.0, 53.9 | 61.3, 36.5, 88.7, 99.2 | 46.1, 55.4, 57.3 | 72.3, 72.3, 163.3, 120.0 | 100.9, 100.9, 69.5, 120.0 |
| Space group | P6522 | P61 | P4212 | P21 | P212121 | P6522 | H3 |
| Number of molecules/asu | 1 | 1 | 2 | 5 | 2 | 2 | 2 |
| Data Collection | |||||||
| Resolution rangea (Å) | 14.02–1.50 (1.58–1.50) | 50.00–1.70 (1.80–1.70) | 61.55–1.90 (2.00–1.90) | 46.40–1.50 (1.60–1.50) | 39.84–1.11 (1.15–1.11) | 50.00–2.15 (2.23–2.15) | 29.14–1.64 (1.73–1.64) |
| Completenessa (%) | 97.0 (82.3) | 99.7 (98.5) | 100.0 (100.0) | 79.7 (37.0) | 99.4 (100.0) | 100.0 (99.9) | 99.7 (100.0) |
| Multiplicitya | 11.2 (2.5) | 6.2 (3.4) | 9.3 (9.4) | 2.7 (0.8) | 5.1 (4.6) | 8.8 (6.5) | 2.7 (2.7) |
| Rmergea (%) | 13.5 (40.7) | 5.6 (53.2) | 10.9 (69.1) | 4.0 (38.0) | 4.2 (14.4) | 6.1 (92.9) | 5.0 (52.4) |
| 〈I/σ(I)〉a | 15.4 (2.0) | 18.1 (1.9) | 18.4 (4.2) | 17.2 (2.0) | 36.6 (11.0) | 17.6 (1.4) | 7.8 (1.8) |
| Refinement | |||||||
| R factor (%) | 21.2 | 19.2 | 17.3 | 16.3 | 13.1 | 20.9 | 19.6 |
| Rfree (%) | 23.1 | 25.3 | 21.0 | 21.5 | 15.7 | 23.2 | 22.4 |
| Rmsd bond length (Å) [angle (°)] | 0.005 (0.9) | 0.009 (1.2) | 0.011 (1.4) | 0.014 (1.5) | 0.014 (1.7) | 0.016 (1.5) | 0.006 (0.9) |
| PDB ID | 2PKT | 2PA1 | 2V1W | 2UZC | 2Q3G | 2PNT | 2W7R |
a
Values in parentheses are for the highest resolution shell.