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. Author manuscript; available in PMC: 2010 Nov 1.
Published in final edited form as: J Nat Prod. 2009 Nov;72(11):1927–1936. doi: 10.1021/np900444m

Table 4.

13C NMR Dataa (δ, DEPT) for 4, 5, 7, and 10–12

C 4 5 7 10 11 12
1 178.4, CH 178.3, CH 178.3, CH 178.2, CH 178.3, CH 178.3, CH
2 132.2, C 132.1, C 132.1, C 132.0, C 132.1, C 132.0, C
3 122.5, CH 122.6, CH 122.7, CH 122.7, CH 122.8, CH 122.7, CH
4 109.8, CH 109.7, CH 109.7, CH 109.6, CH 109.6, CH 109.7, CH
5 142.3, qC 142.8, C 143.0, C 143.4, C 143.4, C 142.9, C
6 28.1, CH2 28.0, CH2 28.0, CH2 28.0, CH2 28.1, CH2 28.1, CH2
7 26.9, CH2 28.7, CH2 28.7, CH2 28.9, CH2 29.0, CH2 29.0, CH2
8 128.1, CH 29.9-29.0b 29.9-29.0b 29.9-29.4b 29.9-29.4 30.0-29.5b
9 130.3, CH 29.9-29.0b 29.9-29.0b 29.9-29.4b 29.9-29.4 30.0-29.5b
10 25.8, CH2 29.9-29.0b 29.9-29.0b 29.9-29.4b 29.2, CH2c 29.1, CH2
11 127.4, CH 29.9-29.0b 29.9-29.0b 29.9-29.4b 27.4, CH2e 27.5, CH2c
12 130.9, CH 29.9-29.0b 29.9-29.0b 29.9-29.4b 130.4, CHd 130.5, CHd
13 27.4, CH2 29.9-29.0b 29.9-29.0b 29.9-29.4b 129.6, CHd 129.6, CHd
14 29.9-29.0b 29.9-29.0b 29.9-29.0b 29.9-29.4b 27.2, CH2e 27.2, CH2c
15 29.9-29.0b 29.9-29.0b 29.9-29.0b 29.9-29.4b 29.1, CH2c 29.1, CH2
16 29.9-29.0b 29.9-29.0b 29.9-29.0b 29.9-29.4b 29.9-29.4b 30.0-29.5b
17 29.9-29.0b 29.9-29.0b 27.5, CH2 29.9-29.4b 29.9-29.4b 30.0-29.5b
18 29.9-29.0b 29.9-29.0b 128.0, CH 29.9-29.4b 29.9-29.4b 30.0-29.5b
19 29.9-29.0b 27.5, CH2 130.6, CH 29.2, CH2e 29.9-29.4b 30.0-29.5b
20 29.9-29.0b 127.9, CH 25.9, CH2 27.4, CH2c 29.9-29.4b 30.0-29.5b
21 29.9-29.0b 130.6, CH 128.9, CH 130.3, CHd 29.9-29.4b 30.0-29.5b
22 29.9-29.0b 25.9, CH2 129.6, CH 129.6, CHd 29.9-29.4b 30.0-29.5b
23 29.9-29.0b 128.9, CH 27.0, CH2 27.2, CH2c 29.9-29.4b 30.0-29.5b
24 29.9-29.0b 129.5, CH 28.9, CH2 29.1, CH2e 28.8, CH2 30.0-29.5b
25 29.9-29.0b 27.0, CH2 25.6, CH2 29.9-29.4 25.6, CH2 28.9, CH2
26 28.9, CH2 28.9, CH2 17.3, CH2 28.8, CH2 17.3, CH2 25.6, CH2
27 25.6, CH2 25.6, CH2 120.1, C 25.5, CH2 120.0, C 17.4, CH2
28 17.3, CH2 17.3, CH2 17.3, CH2 120.1, C
29 120.0, C 120.1, C 120.0, C
a

Bruker AMX 100 MHz spectrometer; δ values are reported in ppm referenced to CDCl3 (δC 77.23) as internal standard; Numerical order groups compounds of similar chain length;

b

All carbons were CH2;

c,d,e

Values may be interchanged.