Table 5.

¹³C NMR Data^a (δ, DEPT) for 6, 8, 9, and 19–21

C	6	8	9	19	20	21
1	178.3, CH	178.3, CH	178.3, CH	178.3, CH	178.3, CH	178.4, CH
2	132.1, C	132.1, C	132.1, C	132.1, C	132.2, C	132.2, C
3	122.4, CH	122.8, CH	122.6, CH	122.7, CH	122.8, CH	122.8, CH
4	109.7, CH	109.6, CH	109.6, CH	109.6, CH	109.6, CH	109.6, CH
5	142.6, C	143.3, C	142.9, C	143.2, C	142.8, C	143.2, C
6	28.0, CH2	28.1, CH2	28.1, CH2	28.1, CH2	28.1, CH2	28.1, CH2
7	28.7, CH2	29.0, CH2	29.0, CH2	29.2, CH2	29.1, CH2	29.1, CH2
8	29.9-29.0b	29.9-29.5b	30.0-29.4b	29.9-29.5b	29.8-29.3b	29.8-29.4
9	29.9-29.0b	29.9-29.5b	30.0-29.4b	29.9-29.5b	29.8-29.3b	29.8-29.4
10	29.9-29.0b	29.9-29.5b	30.0-29.4b	29.9-29.5b	29.8-29.3b	29.8-29.4
11	29.9-29.0b	29.9-29.5b	30.0-29.4b	29.9-29.5b	29.8-29.3b	29.8-29.4
12	29.9-29.0b	29.9-29.5b	30.0-29.4b	29.9-29.5b	27.4, CH2	29.8-29.4
13	29.9-29.0b	29.9-29.5b	30.0-29.4b	29.9-29.5b	128.0, CH	29.8-29.4
14	29.9-29.0b	29.9-29.5b	30.0-29.4b	27.4, CH2	130.4, CH	27.4, CH2
15	27.5, CH2	29.1, CH2	30.0-29.4b	128.4, CHb	25.8, CH2c	127.9, CH
16	128.0, CH	27.4, CH2c	30.0-29.4b	130.3, CH	128.5, CHd	130.6, CH
17	130.5, CH	130.4, CHd	29.2, CH2e	25.9, CH2	128.4, CHd	25.8, CH2c
18	25.9, CH2	129.6, CHd	27.4, CH2c	128.2, CHb	25.7, CH2c	128.5, CH
19	128.9, CH	27.2, CH2c	130.5, CHd	130.1, CH	127.3, CH	128.5, CH
20	129.5, CH	29.1, CH2	129.8, CHd	29.4, CH2	132.0, CH	25.7, CH2c
21	27.0, CH2	29.9-29.5b	27.2, CH2c	23.0, CH2	20.8, CH2	127.3, CH
22	28.9, CH2	28.9, CH2	29.1, CH2e	14.0, CH3	14.5, CH3	132.0, CH
23	25.6, CH2	25.6, CH2	30.0-29.4b			20.8, CH2
24	17.4, CH2	17.3, CH2	28.9, CH2			14.5, CH3
25	120.1, C	120.0, C	25.6, CH2
26			17.3, CH2
27			120.0, C

^aBruker AMX 100 MHz spectrometer; δ values are reported in ppm referenced to CDCl₃ (δ_C 77.23) as internal standard; Numerical order groups compounds of similar chain length.

^bAll carbons were CH₂;

^c,d,eValues may be interchanged.