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Synthesis of HDP-P-AraG. Reagents: (a) see Reference 1; (b) 1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane, pyridine; (c) trifluoromethanesulfonic acid, pyridine; (d) LiOAc, N,N-DMF; (e) tetrabutylammonium fluoride, HOAc, CH3CN; (f) hexadecyloxypropyl phosphate, dicyclohexylcarbodiimide, pyridine; and (g) three deprotection steps.
