Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
Prins fluorination microwave (100 W, 50 °C, 10 min) reactions using homoallylic alcohol (3), an aldehyde and BF3·OEt2 in DCM.
 | |||
| entry | aldehyde | d.r. (5/6) | conversion |
| 5a | 4-nitrobenzaldehyde | 1.5/1 | 53% |
| 5e | 2-bromobenzaldehyde | 3/1 | 92% |
| 5f | 3-bromobenzaldehyde | 1.8/1 | 93% |
| 5g | 4-bromobenzaldehyde | 2.3/1 | 83% |
| 5i | 4-methoxybenzaldehyde | 1/1.2 | 41% |
| 5k | hexanal | 1.8/1 | 91% |
| 5m | benzaldehyde | 3.4/1 | 66% |
