Table 2.
Changes of the polymerization level calculated from integrated α-H peak area of polymerized SNS and the integrated α- H area of SNS monomer (integrated from 670 cm-1 to 710 cm-1) in respect to polymerization time. Three sets of time-dependant in-situ electropolymerization of SNS are presented (experiment 1 -3). The peak area change of the polymerization levels are presented in %.
Polymerization time [min] | α-H polySNS vs. SNS peak area change [%] Exp. 1 | α-H polySNS vs. SNS peak area change [%] Exp. 2 | α-H polySNS vs. SNS peak area change [%] Exp. 3 |
---|---|---|---|
5 | 2.78 | 3.19 | 5.72 |
10 | 8.64 | 9.31 | 13.4 |
20 | 15.7 | 17.1 | 21.2 |
30 | 19.1 | 23.4 | 26.5 |