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. Author manuscript; available in PMC: 2011 Apr 15.
Published in final edited form as: Anal Chem. 2010 Apr 15;82(8):3139–3145. doi: 10.1021/ac9027802

Table 2.

Changes of the polymerization level calculated from integrated α-H peak area of polymerized SNS and the integrated α- H area of SNS monomer (integrated from 670 cm-1 to 710 cm-1) in respect to polymerization time. Three sets of time-dependant in-situ electropolymerization of SNS are presented (experiment 1 -3). The peak area change of the polymerization levels are presented in %.

Polymerization time [min] α-H polySNS vs. SNS peak area change [%] Exp. 1 α-H polySNS vs. SNS peak area change [%] Exp. 2 α-H polySNS vs. SNS peak area change [%] Exp. 3
5 2.78 3.19 5.72
10 8.64 9.31 13.4
20 15.7 17.1 21.2
30 19.1 23.4 26.5