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. Author manuscript; available in PMC: 2010 Jul 6.
Published in final edited form as: Inorg Chem. 2009 Jul 6;48(13):6159–6166. doi: 10.1021/ic900494u

Figure 4.

Figure 4

Structures and metric comparisons of [Ni(pmdt)(SH)]1− (3) and [Ni(pdtc)(SH)]1− (12). Metric data (Å; deg) for 3/12: Ni-S(1,2) 2.165(1), 2.202(1)/2.172(1), 2.181(1); Ni-N 1.904(3)/1.893(1); Ni-S(3) 2.192(1)/2.166(1) Å; N(1)-Ni-S(1,2) 88.73(9), 88.28(9)/88.71(4), 88.54(5); S(3)-Ni-S(1,2) 92.08(4), 91.16(4)/92.95(1), 89.93(2); S(1)-Ni-S(2) 173.11(4)/176.25(2); N(1)-Ni-S(3) 177.64(9)/176.21(4)°.