Table 1.
sIL-10R2 Data Collection, Phasing, and Refinement Statistics
Crystal 1 | Crystal 2 | |
---|---|---|
Space group | P6 | P6 |
Cell a,b | 124.27 | 124.84 |
Cell c | 83.70 | 84.22 |
Wavelength (Å) | 0.97934 (peak) | 1.00000 |
Resolution | 50–2.5 | 50–2.14 |
Highest resolution | 2.59–2.50 | 2.22–2.14 |
Completeness (%) | 100 (100) | 97.5 (84.6) |
Redundancy | 10.8 (10.7) | 11.0 (5.1) |
I/σ | 72 (26) | 50 (5.9) |
Rsym (%) | 7.1 (15.7) | 7.1 (28.9) |
Phasing statistics | ||
# Se (SOLVE) | 12 | |
FOM (SOLVE) | 0.48 | |
FOM (CNS DM) | 0.91 | |
Refinement statistics | ||
Resolution (Å) | 50–2.14 | |
Highest resolution | 2.14–2.16 | |
Rwork (%) | 21.0 (27.7) | |
No. of reflections (work) | 38,362 | |
Rfree (%) | 23.9 (36.5) | |
No. of reflections (free) | 2,016 | |
Residues in model | A: 20–220 | |
B: 20–215 | ||
No. of protein atoms | 3,284 | |
No. of water atoms | 212 | |
No. of sulfate | 10 | |
No. of glycerol | 1 | |
Rmsd bond distance (Å) | 0.0085 | |
Rmsd bond angles (°) | 1.43 | |
Average B factor (Å2) | 37.3 | |
Ramachandran plot | ||
Most favored (%) | 88.1 | |
Additionally allowed (%) | 9.6 | |
Generally allowed (%) | 1.4 | |
Disallowed (%) | 0.8 |