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. 2010 May 27;66(Pt 6):750–754. doi: 10.1107/S174430911001376X

Table 2. Data-collection statistics at pH 6.5.

Precipitant Asp Glu Arg Orn Lys GlyEE
Growth pH 6.5 6.5 6.5 6.5 6.5 6.5
Unit-cell parameters            
a (Å) 78.41 78.76 77.28 78.74 78.60 78.94
c (Å) 37.36 36.82 38.04 37.08 37.01 37.11
Unit-cell volume (Å3) 2.30 × 105 2.28 × 105 2.27 × 105 2.30 × 105 2.29 × 105 2.31 × 105
Resolution (Å) 19.60–1.70 30.71–2.20 31.22–1.90 30.86–1.80 31.22–1.90 19.15–1.40
Wavelength (Å) 0.90 1.54 1.54 1.54 0.90 0.90
Crystal-to-detector distance (mm) 200 100 100 100 200 200
Oscillation angle (°) 2.0 3.0 2.0 2.0 2.0 2.0
Exposure time (s per frame) 1.0 210 210 210 1.0 1.0
Total oscillation range (°) 80 120 100 100 80 80
No. of reflections            
 Observed 82829 45201 68417 79663 98154 146461
 Unique 13325 6200 9256 11203 14715 23381
Completeness (%) 99.9 (100.0) 98.8 (92.9) 97.6 (98.6) 99.1 (94.5) 93.5 (95.9) 99.0 (99.9)
Rmerge 0.109 (0.276) 0.081 (0.169) 0.068 (0.380) 0.049 (0.201) 0.121 (0.260) 0.115 (0.294)
I/σ(I) 16.1 (6.5) 19.2 (7.5) 19.2 (4.4) 26.9 (7.9) 15.7 (7.3) 14.4 (5.5)

R merge = Inline graphic Inline graphic, where I i(hkl) is the intensity of the ith observation and 〈I(hkl)〉 is the mean intensity of the reflection.