Table 2. Data-collection statistics at pH 6.5.
| Precipitant | Asp | Glu | Arg | Orn | Lys | GlyEE |
|---|---|---|---|---|---|---|
| Growth pH | 6.5 | 6.5 | 6.5 | 6.5 | 6.5 | 6.5 |
| Unit-cell parameters | ||||||
| a (Å) | 78.41 | 78.76 | 77.28 | 78.74 | 78.60 | 78.94 |
| c (Å) | 37.36 | 36.82 | 38.04 | 37.08 | 37.01 | 37.11 |
| Unit-cell volume (Å3) | 2.30 × 105 | 2.28 × 105 | 2.27 × 105 | 2.30 × 105 | 2.29 × 105 | 2.31 × 105 |
| Resolution (Å) | 19.60–1.70 | 30.71–2.20 | 31.22–1.90 | 30.86–1.80 | 31.22–1.90 | 19.15–1.40 |
| Wavelength (Å) | 0.90 | 1.54 | 1.54 | 1.54 | 0.90 | 0.90 |
| Crystal-to-detector distance (mm) | 200 | 100 | 100 | 100 | 200 | 200 |
| Oscillation angle (°) | 2.0 | 3.0 | 2.0 | 2.0 | 2.0 | 2.0 |
| Exposure time (s per frame) | 1.0 | 210 | 210 | 210 | 1.0 | 1.0 |
| Total oscillation range (°) | 80 | 120 | 100 | 100 | 80 | 80 |
| No. of reflections | ||||||
| Observed | 82829 | 45201 | 68417 | 79663 | 98154 | 146461 |
| Unique | 13325 | 6200 | 9256 | 11203 | 14715 | 23381 |
| Completeness (%) | 99.9 (100.0) | 98.8 (92.9) | 97.6 (98.6) | 99.1 (94.5) | 93.5 (95.9) | 99.0 (99.9) |
| Rmerge† | 0.109 (0.276) | 0.081 (0.169) | 0.068 (0.380) | 0.049 (0.201) | 0.121 (0.260) | 0.115 (0.294) |
| I/σ(I) | 16.1 (6.5) | 19.2 (7.5) | 19.2 (4.4) | 26.9 (7.9) | 15.7 (7.3) | 14.4 (5.5) |
R
merge =
, where I
i(hkl) is the intensity of the ith observation and 〈I(hkl)〉 is the mean intensity of the reflection.