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. Author manuscript; available in PMC: 2010 Jun 15.
Published in final edited form as: J Phys Chem B. 2007 Oct 17;111(44):12865–12875. doi: 10.1021/jp072156s

Table 6.

Best-fit parameters obtained with combined fitting of 5 relaxation rates (2H T1, T2 and the three relaxation rates associated with the rank 2 coherences) acquired at 11.7 T, 35 °C, for the depicted methyl groups. The global motion correlation time used was τm = 2.55 ns.12,43 Note that all the c22c02 values are negative except for c22c02 of L38δ1, marked with an asterisk.

Methyl c02 c22 RC τ0, ps c22c02
L8δ1 1.49 –0.50 0.017 43 0.36
L38δ1 –0.54 –0.56 0.015 38 1.04*
L56δ2 1.46 –0.50 0.020 51 0.34
T55 1.99 –0.66 0.037 94 0.33
T23 2.17 –0.63 0.029 71 0.29
A18 2.09 –0.74 0.039 100 0.35
A50 2.41 –0.55 0.026 66 0.23
L38δ2 1.19 –0.52 0.016 41 0.44
T37 1.89 –0.58 0.032 82 0.31
T17 1.61 –0.54 0.040 102 0.30
T3 2.12 –0.62 0.030 122 0.29
V49γ2 1.83 –0.51 0.021 54 0.28
A6 2.06 –0.80 0.042 107 0.39
A61 1.67 –0.51 0.024 61 0.31
V47γ1 1.59 –0.51 0.029 74 0.32
V2γ2 1.75 –0.94 0.058 147 0.54
I9g 1.88 –0.90 0.044 112 0.41
A31 1.91 –0.92 0.044 112 0.48