. Author manuscript; available in PMC: 2010 Jul 1.

Published in final edited form as: J Comb Chem. 2009 Jul–Aug;11(4):617–625. doi: 10.1021/cc9000357

Table 3.

Yield and purity data for chemset 7.

Chemset 7	%Yield	LCMS purity	NMR purity
{1,1}	36	87	93
{2,1}	54	82	–^a
{3,1}	70	82	–^a
{1,2}	45	90	94
{2,2}	38	82	–^a
{3,2}	66	89	–^a
{1,3}	70	87	–^a
{2,3}	58	86	–^a
{3,3}	61	88	96
{1,4}	50	80	–^a
{2,4}	49	69	–^a
{3,4}	57	88	–^a
{1,5}	40	93	99
{2,5}	50	100	94
{3,5}	26	88	–^a
{1,6}	29	86	91
{2,6}	60	83	–^a
{3,6}	75	88	–^a
{1,7}	33	85	–^a
{2,7}	65	100	98
{3,7}	61	90	–^a
{1,8}	63	85	–^a
{2,8}	45	98	96
{3,8}	56	94	–^a
{1,9}	68	91	–^a
{2,9}	57	85	–^a
{3,9}	66	98	96
{1,10}	70	94	–^a
{2,10}	26	84	–^a
{3,10}	65	80	96
{1,11}	61	90	91
{2,11}	47	84	–^a
{3,11}	54	86	–^a
{1,12}	46	79	–^a
{2,12}	55	87	–^a
{3,12}	56	88	91
{1,13}	51	84	–^a
{2,13}	58	81	–^a
{3,3}	75	90	99
{114}	60	84	-
{2,14}	63	78	-
{3,14}	74	88	96
{1,15}	–^b	-	-
{2,15}	–^b	-	-
{3,15}	29	87	–^a
{1,16}	79	83	–^a
{2,16}	60	100	94
{3,16}	51	85	–^a
{1,17}	63	100	96
{2,17}	56	59	–^a
{3,17}	76	88	–^a
{1,18}	17	100	–^a
{2,18}	71	93	–^a
{3,18}	45	94	–^a
{1,19}	70	92	–^a
{2,19}	49	100	93
{3,19}	70	89	–^a
{1,20}	66	88	–^a
{2,20}	60	100	97
{3,20}	36	89	–^a
{1,21}	41	88	–^a
{2,21}	48	81	–^a
{3,21}	13	95	–^a
{1,22}	69	92	94
{2,22}	52	84	90
{3,22}	21	93	–^a

Data not obtained

No product obtained