Skip to main content
. Author manuscript; available in PMC: 2011 Jun 18.
Published in final edited form as: Org Lett. 2010 Jun 18;12(12):2864–2867. doi: 10.1021/ol100996w

Table 1.

Scope of Aldehyde Glyoxylation

graphic file with name nihms207404u2.jpg
entry product structure yielda (%)
1 4a graphic file with name nihms207404t1.jpg 87
2 4b graphic file with name nihms207404t2.jpg 92
3 4c graphic file with name nihms207404t3.jpg 80
4 4d graphic file with name nihms207404t4.jpg 86
5 4e graphic file with name nihms207404t5.jpg 89
6 4f graphic file with name nihms207404t6.jpg 90
7 4g graphic file with name nihms207404t7.jpg 92
8 4h graphic file with name nihms207404t8.jpg 85
9 4i graphic file with name nihms207404t9.jpg 86
10 4j graphic file with name nihms207404t10.jpg 88
11b 4k graphic file with name nihms207404t11.jpg 96
12b 4l graphic file with name nihms207404t12.jpg 85
a

Yields of analytically pure material after work-up.

b

Sm(OiPr)3 (10 mol %) was employed.