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. Author manuscript; available in PMC: 2010 Jun 28.
Published in final edited form as: Org Lett. 2005 Sep 1;7(18):3917–3920. doi: 10.1021/ol051372l

Table 1.

Cycloaddition of Arynes and Conjugated Enynes

graphic file with name nihms-214843-t0004.jpg

entry cycloaddition substrate cycloaddition product % yieldb
1 graphic file with name nihms-214843-t0005.jpg graphic file with name nihms-214843-t0006.jpg 74
2 graphic file with name nihms-214843-t0007.jpg graphic file with name nihms-214843-t0008.jpg 24
3 graphic file with name nihms-214843-t0009.jpg graphic file with name nihms-214843-t0010.jpg 66
4 graphic file with name nihms-214843-t0011.jpg graphic file with name nihms-214843-t0012.jpg 24
5 graphic file with name nihms-214843-t0013.jpg graphic file with name nihms-214843-t0014.jpg 46
6 graphic file with name nihms-214843-t0015.jpg graphic file with name nihms-214843-t0016.jpg 61
a

Tetrabutylammonium triphenyldifluorosilicate (n-Bu4NSiPh3F2).

b

Isolated yields of products purified by column chromatography.