Table 1.
entry | cycloaddition substrate | cycloaddition product | % yieldb |
---|---|---|---|
1 | 74 | ||
2 | 24 | ||
3 | 66 | ||
4 | 24 | ||
5 | 46 | ||
6 | 61 |
Tetrabutylammonium triphenyldifluorosilicate (n-Bu4NSiPh3F2).
Isolated yields of products purified by column chromatography.
entry | cycloaddition substrate | cycloaddition product | % yieldb |
---|---|---|---|
1 | 74 | ||
2 | 24 | ||
3 | 66 | ||
4 | 24 | ||
5 | 46 | ||
6 | 61 |
Tetrabutylammonium triphenyldifluorosilicate (n-Bu4NSiPh3F2).
Isolated yields of products purified by column chromatography.