Table 1.
No. | δ c | δH (J in Hz) |
---|---|---|
1 | 34.3 CH2 | 2.27 (2H, m) |
2 | 17.7 CH2 | 1.44 (2H, m) |
3 | 41.6 CH2 | 1.41 (2H, m) |
4 | 32.8 C | --- |
5 | 56.7 CH | 0.83 (1H, m) |
6 | 18.3 CH2 | 1.34 (2H, m) |
7 | 41.9 CH2 | 1.76 (2H, m) |
8 | 37.3 C | --- |
9 | 58.5 CH | 0.87 (1H, m) |
10 | 42.0 C | --- |
11 | 29.8 CH2 | 1.86 (2H, m) |
12 | 81.8 CH | 3.46 (1H, m) |
13 | 43.9 C | --- |
14 | 52.9 CH | 1.08 (1H, m) |
15 | 23.2 CH2 | 2.22 (2H, m) |
16 | 143.0 CH | 7.03 (1H, s) |
17 | 138.6 C | --- |
18 | 61.3 CH | 3.22 (1H, s) |
19 | 33.7 CH3 | 0.80 (3H, s) |
20 | 21.7 CH3 | 0.71 (3H, s) |
21 | 16.4 CH3 | 1.05 (3H, s) |
22 | 62.1 CH2 | 3.77 (1H, d,11.4) 3.95 (1H, d, 11.4) |
23 | 9.6 CH3 | 0.76 (3H, s) |
24 | 199.1 C | --- |
25 | 204.4 CH | 9.75 (1H, s) |
26 | 25.0 CH3 | 2.24 (3H, s) |
CDCl3; 150 MHz for 13C; 600 MHz for 1H.