Table 1.
Space group | P61 |
Molecules in asymmetric unit | 2 |
Cell axes (Å) and angles (°) | 210.9 210.9 115.3, 90 90 120 |
X-ray source, beamline, wavelength (Å) | ESRF, ID-14-4, 0.93 |
Temperature | 100°K |
Diffraction limits (Å) | 31.1–3.2 |
Number of measured reflections | 482,340 |
Number of unique reflections | 47,979 |
Mosaicity (°) | 0.25 |
Multiplicity | 5.5 |
Completeness: all data (highest shell*) | 99.9 % (100 %) |
Rsym: all data (highest shell) | 8.3% (47.5 %) |
I/sigma: all data (highest shell) | 15.1 (3.5) |
Highest resolution shell is 3.31–3.2 Å.