Table 3.
Bond angles (deg) in 2
S(3)–Mo(1)–S(2) | 141.97(5) | S(4)–Mo(2)–Mo(1) | 87.94(4) |
S(3)–Mo(1)–S(1) | 133.77(5) | S(3)–Mo(2)–Mo(1) | 143.40(3) |
S(2)–Mo(1)–S(1) | 84.26(4) | C(11)–S(3)–Mo(1) | 97.78(18) |
S(3)–Mo(1)–Mo(2) | 124.18(3) | C(11)–S(3)–Mo(2) | 95.75(17) |
S(2)–Mo(1)–Mo(2) | 76.36(4) | Mo(1)–S(3)–Mo(2) | 92.09(4) |
S(1)–Mo(1)–Mo(2) | 51.17(3) | C(2)–S(1)–Mo(2) | 107.43(17) |
S(1)–Mo(2)–S(4) | 142.39(5) | C(2)–S(1)–Mo(1) | 94.47(17) |
S(1)–Mo(2)–S(3) | 130.19(4) | Mo(2)–S(1)–Mo(1) | 73.06(4) |
S(4)–Mo(2)–S(3) | 84.17(4) | C(1)–S(2)–Mo(1) | 102.66(19) |
S(1)–Mo(2)–Mo(1) | 55.77(3) | C(12)–S(4)–Mo(2) | 103.05(18) |