Table 3.
Entry | Substrate | Product | 2, %a,b |
---|---|---|---|
1 | 2f, 79 | ||
2 | 2g, 91 | ||
3 | 2h, 91c | ||
4 | 2i, 48d | ||
5 | 2j, 65e | ||
6 | 2k, 71f | ||
7 | 2l, 68 | ||
8 | 2m, 77 | ||
9 | 2n, 67 |
Isolated yield of product for reactions performed on 0.5 mmol scale.
2f and 2l contained 8 and 6% of the corresponding desilylated furan, respectively.
14:1 ratio of 2h:3h.
10:1 ratio of 2i:3i.
8:1 ratio of 2j:3j.
GC Yield, 2k is a volatile compound.