Table 1. Data-collection statistics.
Beamline | 08ID-1, Canadian Light Source |
Detector | MAR 300 CCD |
Temperature (K) | 100 |
Space group | P212121 |
Unit-cell parameters (Å) | a = 80.23, b = 124.90, c = 164.80 |
Resolution range (Å) | 50–3.20 (3.28–3.20) |
Matthews coefficient (Å3 Da−1) | 2.58 |
Solvent content (%) | 52 |
No. of molecules in asymmetric unit | 4 |
No. of measured reflections | 193080 (12759) |
Total No. of unique reflections | 26008 (1708) |
Completeness (%) | 92.9 (84.6) |
Multiplicity | 7.42 (7.47) |
Rmerge | 0.22 (0.81) |
〈I/σ(I)〉 | 10.06 (2.68) |