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. 2010 Jun 24;66(Pt 7):851–853. doi: 10.1107/S1744309110020130

Table 1. Crystal data and data-collection statistics.

Values in parentheses are for the highest resolution shell.

Space group P1
Unit-cell parameters (Å, °) a = 15.08, b = 22.75, c = 30.20, α = 96.9, β = 103.1, γ = 96.5
Matthews coefficient (Å3 Da−1) 2.48
Solvent content (%) 50.4
No. of protomers per asymmetric unit 1
Temperature (K) 100
X-ray wavelength (Å) 1.54
Oscillation range (°) 1.0
Crystal-to-detector distance (mm) 70
Resolution range (Å) 50–1.43 (1.45–1.43)
Completeness (%) 88.5 (69.4)
Rmerge (%) 2.3 (4.3)
Mean I/σ(I) 44.6 (38.1)
Redundancy 3.8 (3.0)

R merge = Inline graphic Inline graphic, where 〈I(hkl)〉 is the mean intensity of symmetry-equivalent reflections.