Table 1. Crystal data and data-collection statistics.
Space group | P1 |
Unit-cell parameters (Å, °) | a = 15.08, b = 22.75, c = 30.20, α = 96.9, β = 103.1, γ = 96.5 |
Matthews coefficient (Å3 Da−1) | 2.48 |
Solvent content (%) | 50.4 |
No. of protomers per asymmetric unit | 1 |
Temperature (K) | 100 |
X-ray wavelength (Å) | 1.54 |
Oscillation range (°) | 1.0 |
Crystal-to-detector distance (mm) | 70 |
Resolution range (Å) | 50–1.43 (1.45–1.43) |
Completeness (%) | 88.5 (69.4) |
Rmerge† (%) | 2.3 (4.3) |
Mean I/σ(I) | 44.6 (38.1) |
Redundancy | 3.8 (3.0) |
R merge = , where 〈I(hkl)〉 is the mean intensity of symmetry-equivalent reflections.