TABLE 3.
Calculations
% Fully Synthesized Product : {(b)/(b+c+a)} * 100 |
Where, “b” is the fully synthesized product, “c” are the intermediate synthesis products and “a” is the remaining unsynthesized substrate. |
% Cleaved Product : {(b)/(b+a)} * 100 |
Where, “b” is the cleaved product and “a” is the remaining uncleaved substrate. |
% Ligated Product: {(b)/(b+a)} * 100 |
Where, “b” is the ligated product and “a” is the remaining unligated substrate. |
% Bound Product: {(b)/(b+a)} * 100 |
Where, “b” is the bound product and “a” is the remaining unbound substrate. |
% Unwound Product: {(b)/(b+a)} * 100 |
Where, “b” is the unwound product and “a” is the remaining unwound substrate Strand Melting is measured in a similar manner. |
% Annealed Product: {(b)/(b+a)} * 100 |
Where, “b” is the annealed product and “a” is the remaining unannealed substrate |
Calculation of Dissociation Constants: After EMSA, the curves are fit using nonlinear least square regression of the hyperbolic equation: |
y = Bmax*[Protein]/(Kd + [Protein]) |
where, y is the percent of the oligonucleotide bound, [Protein] is the concentration of protein in nM, Bmax is the maximum binding and Kd is the equilibrium dissociation constant. |