Table 5.
Selected bond lengths (Å) and bond angles (°) for 6
| Bond lengths | |||
| Re(1)–O(1) | 1.696(6) | Re(1)–N(1) | 2.026(11) |
| Re(1)–O(3) | 1.991(7) | Re(1)–O(2) | 2.035(6) |
| Re(1)–O(4) | 1.998(6) | Re(1)–N(2) | 2.093(8) |
| Bond angles | |||
| O(1)–Re(1)–O(3) | 102.8(3) | O(4)–Re(1)–O(2) | 81.5(3) |
| O(1)–Re(1)–O(4) | 171.6(3) | N(1)–Re(1)–O(2) | 90.7(7) |
| O(3)–Re(1)–O(4) | 84.9(3) | O(1)–Re(1)–N(2) | 94.6(3) |
| O(1)–Re(1)–N(1) | 100.6(3) | O(3)–Re(1)–N(2) | 89.1(3) |
| O(3)–Re(1)–N(1) | 84.0(7) | O(4)–Re(1)–N(2) | 82.0(3) |
| O(4)–Re(1)–N(1) | 83.4(3) | N(1)–Re(1)–N(2) | 164.3(4) |
| O(1)–Re(1)–O(2) | 91.0(3) | O(2)–Re(1)–N(2) | 92.7(3) |
| O(3)–Re(1)–O(2) | 165.9(3) | ||