Table II.
Size, Shape, Weight, Zn Content, WL, MC, EE, and L of the Beads (Data Represents Mean ± SD (N = 3))
Variables | Values | Shape (ER)v | Size (µm)v | Weight of 50 beads (mg)v | Zn content (µg mg−1 bead) | MC (%) | EE (%) |
---|---|---|---|---|---|---|---|
Cross-linking agent | Zn | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92 | 10.09 ± 0.43k | 97.99 ± 0.10k |
Ca | 1.07 ± 0.05 | 1,077.77 ± 72.97 | 32.62 ± 0.77 | – | 16.16 ± 1.00 | 98.65 ± 0.21 | |
Cross-linking pH | 1.5 | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92a | 10.09 ± 0.43 | 97.99 ± 0.10 |
6.3 | 1.06 ± 0.03 | 1,111.76 ± 40.61 | 24.49 ± 0.14 | 81.73 ± 0.94 | 11.05 ± 0.76 | 97.77 ± 0.68 | |
Zinc acetate concentration (%) | 1 | 1.03 ± 0.01 | 881.09 ± 38.29 | 19.84 ± 0.08 | 33.55 ± 0.87b | 6.29 ± 0.95b | 98.29 ± 0.12q |
2.5 | 1.07 ± 0.02 | 886.96 ± 9.81 | 22.83 ± 0.11 | 50.44 ± 2.78 | 9.51 ± 0.66 | 98.01 ± 0.18 | |
5 | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92 | 10.09 ± 0.43 | 97.99 ± 0.10 | |
10 | 1.06 ± 0.02 | 1,035.16 ± 43.22 | 25.54 ± 0.46 | 88.80 ± 0.60c | 11.23 ± 0.79 | 97.68 ± 0.27 | |
Cross-linking time (h) | 0.25 | 1.13 ± 0.07 | 894.28 ± 14.38 | 20.38 ± 0.12 | 42.35 ± 2.94d | 7.78 ± 0.19l | 98.38 ± 0.04r |
0.5 | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92 | 10.09 ± 0.43m | 97.99 ± 0.10s | |
2 | 1.07 ± 0.07 | 920.48 ± 14.47 | 23.24 ± 0.05 | 75.29 ± 0.96 | 12.25 ± 0.79 | 97.06 ± 0.85 | |
24 | 1.10 ± 0.08 | 943.97 ± 15.04 | 24.74 ± 0.24 | 84.00 ± 0.91 | 13.21 ± 0.12 | 96.29 ± 0.11 | |
Drying | RT | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92e | 10.09 ± 0.43e | 97.99 ± 0.10 |
37°C | 1.06 ± 0.03 | 895.76 ± 11.13 | 22.03 ± 0.73 | 54.65 ± 0.65f | 9.56 ± 0.72f | 97.99 ± 0.10 | |
50°C | 1.06 ± 0.03 | 886.88 ± 7.820 | 20.95 ± 0.51 | 85.30 ± 0.42 | 1.45 ± 0.45 | 97.99 ± 0.10 | |
FD | 1.06 ± 0.03 | 2,040.51 ± 46.66 | 19.59 ± 0.05 | 87.76 ± 0.61 | 0.66 ± 0.23 | 97.99 ± 0.10 | |
Pectin concentration (%) | 3 | 1.09 ± 0.03 | 892.87 ± 13.27 | 23.38 ± 0.98 | 116.25 ± 1.18g | 10.70 ± 1.44 | 97.44 ± 0.08t |
4 | 1.07 ± 0.03 | 898.47 ± 16.83 | 22.06 ± 0.55 | 96.02 ± 0.86h | 11.01 ± 0.78 | 97.05 ± 0.09 | |
5 | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92 | 10.09 ± 0.43 | 97.99 ± 0.10 | |
6 | 1.08 ± 0.03 | 907.63 ± 20.25 | 23.81 ± 0.18 | 53.43 ± 2.84 | 10.24 ± 0.72 | 97.75 ± 0.05 | |
Pectin–Resveratrol | 1:1 | 1.07 ± 0.03 | 1140.67 ± 80.12 | 40.16 ± 0.42 | 45.95 ± 2.05 | 15.07 ± 0.49n | 99.28 ± 0.10u |
2:1 | 1.07 ± 0.04 | 993.01 ± 48.82 | 31.57 ± 0.42 | 51.63 ± 2.10 | 12.43 ± 0.24o | 98.55 ± 0.02 | |
3:1 | 1.06 ± 0.03 | 896.44 ± 7.90 | 23.12 ± 0.03 | 54.12 ± 1.92 | 10.09 ± 0.43p | 97.99 ± 0.10 | |
4:1 | 1.05 ± 0.03 | 891.37 ± 11.06 | 21.81 ± 0.20 | 92.33 ± 0.24i | 9.09 ± 0.07 | 97.50 ± 0.03 | |
Blank | – | 1.04 ± 0.01 | 866.62 ± 23.17 | 21.02 ± 0.09 | 111.58 ± 6.60j | 8.54 ± 0.17 | – |
a p < 0.05 between cross-linking pH 1.5 and 6.3
b p < 0.05 between zinc acetate concentration 1% with 2.5%, 5%, and 10%
c p < 0.05 between zinc acetate concentration 10% with 2.5% and 5%
d p < 0.05 among cross-linking time 0.25, 0.5, 2, and 24 h
e p < 0.05 between drying at RT with 50°C and FD
f p < 0.05 between drying at 37°C with 50°C and FD
g p < 0.05 between pectin concentration 3% with 4%, 5%, and 6%
h p < 0.05 between pectin concentration 4% with 5% and 6%
i p < 0.05 between pectin to resveratrol ratio 4:1 with 1:1, 2:1, and 3:1
j p < 0.05 between blank beads with pectin to resveratrol ratio 1:1, 2:1, 3:1, and 4:1
k p < 0.05 between cross-linking agent Ca and Zn
l p < 0.05 between cross-linking time 0.25 h with 0.5, 2, and 24 h
m p < 0.05 between cross-linking time 0.5 h with 2 and 24 h
n p < 0.05 between pectin to resveratrol ratio 1:1 with 2:1, 3:1, 4:1, and blank
o p < 0.05 between pectin to resveratrol ratio 2:1 with 3:1, 4:1, and blank
p p < 0.05 between pectin to resveratrol ratio 3:1 with 4:1 and blank
q p < 0.05 between zinc acetate concentration 1% and 10%
r p < 0.05 between cross-linking time 0.25 h with 2 and 24 h
s p < 0.05 between cross-linking time 0.5 and 24 h
t p < 0.05 among pectin concentration 3%, 4%, 5%, and 6%
u p < 0.05 among pectin to resveratrol ratio 1:1, 2:1, 3:1, and 4:1
vStatistical analysis is not shown