Table 2.

Crosspeaks in 2D NCOCX spectrum of HET-s(218) fibrils.

NCOCX crosspeak number	15N shift (ppm)	13C shift (ppm)	εN (ppm)	εC (ppm)	nmax	possible residue types	final assignment (1-72 numbering)	final assignment (standard numbering)
1	119.0	54.0	0.3	0.15	1	A	30	A247
2	120.5	52.9	0.3	0.15	1	A	31	A248
3	118.1	51.1	0.3	0.15	1	A	20	A237
4	123.1	47.4	0.3	0.15	1	A	11	A228
5	118.8	49.9	0.3	0.15	1	N	9	N226
6	117.3	50.3	0.3	0.15	1	N	45	N262
7	120.4	49.7	0.3	0.15	1	DN	62	N279
8	122.5	49.3	0.3	0.15	1	DN	26	N243
9	116.7	51.7	0.3	0.15	1	EQ	17	E234
10	128.4	52.4	0.3	0.15	1	EQ	63	E280
11	112.9	57.4	0.3	0.15	1	EQ	48	E265
12	122.6	56.7	0.3	0.15	1	EQ	18	E235
13	116.2	52.1	0.3	0.15	1	EQ	55	E272
14	131.3	50.8	0.3	0.15	1	EQKR	23	Q240
15	128.3	46.4	0.3	0.15	1	G	54	G271
16	121.3	42.5	0.3	0.15	1	G	52	G269
17	114.3	41.9	0.3	0.15	1	G	61	G278
18	109.9	41.7	0.3	0.15	1	G	25	G242
19	113.7	44.1	0.3	0.15	1	G	65	G282
20	117.6	41.7	0.3	0.15	1	G	66	G283
21	123.5	42.3	0.3	0.15	1	G	68**	G285**
22	119.8	43.3	0.3	0.15	1	G	36**	G253**
23	129.6	58.9	0.3	0.15	1	I	14	I231
24	111.2	56.8	0.3	0.15	1	I	60	I277
25	117.9	57.5	0.3	0.15	1	K	12	K229
26	115.2	52.2	0.3	0.15	1	K	53	K270
27	113.4	50.8	0.3	0.15	1	L	24	L241
28	130.0	50.6	0.3	0.15	1	L	59	L276
29	122.4	51.2	0.3	0.15	1	LDNF	13	D230
30	125.4	52.6	0.3	0.15	1	R	19	R236
31	117.8	57.1	0.3	0.15	1	S	56	S273
32	124.9	54.3	0.3	0.15	1	S	46	S263
33	122.7	54.7	0.3	0.15	1	S	10	S227
34	108.6	55.2	0.3	0.15	1	not AGT	67**	K284**
35	120.9	60.4	0.3	0.15	1	T	29	T246
36	127.8	59.2	0.3	0.15	1	T	44	T261
37	124.1	58.9	0.3	0.15	1	T	49	T266
38	119.8	57.5	0.3	0.15	1	T	16	T233
39	123.6	64.2	0.3	0.15	1	T	43	T260
40	126.4	57.9	0.3	0.15	1	V	22	V239
41	130.1	58.3	0.3	0.15	1	V	58	V275
42	128.1	58.7	0.3	0.15	1	V	50	V267
43	126.9	55.1	0.3	0.15	1	V	47	V264
44	113.1	59.1	0.3	0.15	1	V	51	V268
45	128.8	60.0	0.3	0.15	1	V	27	V244
46	116.3	59.0	0.3	0.15	1	V	28	V245
47	113.2	52.2	0.3	0.15	1	EQKR	15	R232
48	122.5	52.5	0.3	0.15	1	EQKR	21	R238
49	122.6	52.9	0.3	0.15	1	EQKR	57	R274
50	110.0	54.0	0.3	0.15	1	Y	64	Y281