Table 2.
| |||
---|---|---|---|
X = | % conv. 1 h | % conv. 2.5 h | % conv. 12 h |
Cl− | 10 | 16 | 70 |
OAc− | 100 | na | na |
CF3CO2− | 7 | 10 | 20 |
ClO4− | 0 | 0 | trace |
SbF6− | 0 | 0 | 0 |
SbF6− + NMM(30%) | 30 | 35 | 86 |
Determined by 1H NMR analysis against an internal standard.
| |||
---|---|---|---|
X = | % conv. 1 h | % conv. 2.5 h | % conv. 12 h |
Cl− | 10 | 16 | 70 |
OAc− | 100 | na | na |
CF3CO2− | 7 | 10 | 20 |
ClO4− | 0 | 0 | trace |
SbF6− | 0 | 0 | 0 |
SbF6− + NMM(30%) | 30 | 35 | 86 |
Determined by 1H NMR analysis against an internal standard.