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. Author manuscript; available in PMC: 2011 Jun 7.

Published in final edited form as: Organometallics. 2010 Jun 7;29(13):2926–2942. doi: 10.1021/om1001827

Molecular structure of 1 as determined by a single crystal X-ray diffraction study. Hydrogen atoms omitted for clarity; thermal ellipsoids set at the 50% probability level. Selected bond lengths are given in Å. Selected bond angles (°): Nb(1)-N(1)-C(1) 163.59(19), Cl(1)-Nb(1)-Cl(2) 160.68(2), N(1)-Nb(1)-N(3) 171.92(8), N(2)-Nb(1)-N(4) 172.98(7).

Molecular structure of 1 as determined by a single crystal X-ray diffraction study. Hydrogen atoms omitted for clarity; thermal ellipsoids set at the 50% probability level. Selected bond lengths are given in Å. Selected bond angles (°): Nb(1)-N(1)-C(1) 163.59(19), Cl(1)-Nb(1)-Cl(2) 160.68(2), N(1)-Nb(1)-N(3) 171.92(8), N(2)-Nb(1)-N(4) 172.98(7).