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. Author manuscript; available in PMC: 2011 Jun 7.
Published in final edited form as: Organometallics. 2010 Jun 7;29(13):2926–2942. doi: 10.1021/om1001827

Figure 5.

Figure 5

The molecular structure of 5 as determined by a single crystal X-ray diffraction study. The hydrogen atoms were omitted for clarity; the thermal ellipsoids were set at the 50% probability level. Selected bond lengths are given in Å. Selected bond angles (°): Nb(1)-N(1)-C(1) 173.27(16), N(1)-Nb(1)-N(2) 103.93(7), N(1)-Nb(1)-N(3) 98.99(7), N(1)-Nb(1)-Cl(2) 107.81(6), N(1)-Nb(1)-Cl(1) 104.00(6), N(2)-Nb(1)-Cl(2) 148.05(5), N(3)-Nb(1)-Cl(1) 156.86(5).