Table 1.
Data collection and structure statistics.
| SeMet-FcsSBP + A-trisaccharide | |
|---|---|
| Data collection | |
| Space Group | P21 |
| Resolution (Å) | 30.00–2.35 (2.48–2.35)* |
| Cell Dimensions | |
| (a, b, c) | 36.9, 104.9, 97.7 |
| (α, β, γ) | 90, 89.95, 90 |
| Rmerge | 0.097 (0.390) |
| I/σI | 22.5 (5.5) |
| Completeness (%) | 100.0 (100.0) |
| Redundancy | 10.4 (10.4) |
| # Reflections | 323208 |
| # unique reflections | 31126 |
| Refinement | |
| Rwork/Rfree | 0.21/0.26 |
| No. atoms | |
| Protein | 2983 (A) 2983 (B) |
| Ligand/ion atoms | 72 (sugar) 2 (IOD) |
| Water molecules | 410 |
| B-factors | |
| Protein | 23.3 (A) 23.3 (B) |
| Ligand/ion | 17.5 (sugar) 41.2 (IOD) |
| Water | 27.6 |
| R.m.s deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (°) | 1.212 |
| Ramachandran statistics (%) | |
| Preferred | 94.3 |
| allowed | 5.5 |
| outliers | 0.1 |
*
Highest resolution shell is shown in parenthesis.