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. Author manuscript; available in PMC: 2010 Jul 30.
Published in final edited form as: Tetrahedron Lett. 2009 Mar 25;50(12):1264–1266. doi: 10.1016/j.tetlet.2008.12.114

Table 1.

Synthesis of γ-iodo ketones13

graphic file with name nihms213708t1.jpg
Substrate Product R R′ Yielda (%)
1a 2a Ph H 79
1b 2b p-CH3O-Ph H 67
1c 2c p-F-Ph H 79
1d 2d Cyclohexyl H 64
1e 2e n-hexyl H 80
1f 2fb p-F-Ph Et 80
a

Isolated yield.

b

Conditions: Reaction run at 0 °C in 20% H2O/MeCN.