Bruker APEXII area-detector diffractometer | 6166 independent reflections |
Radiation source: fine-focus sealed tube | 4469 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.029 |
T = 293(2) K | θmax = 28.2º |
φ and ω scan | θmin = 1.9º |
Absorption correction: multi-scan(SADABS; Bruker, 2004) | h = −14→13 |
Tmin = 0.520, Tmax = 0.665 | k = −21→21 |
19080 measured reflections | l = −19→19 |