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. 2007 Dec 6;64(Pt 1):o1–o2. doi: 10.1107/S160053680706182X
Oxford Diffraction Gemini R CCD diffractometer 8636 independent reflections
Radiation source: fine-focus sealed tube 4667 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.027
Detector resolution: 10.5081 pixels mm-1 θmax = 32.5º
T = 296(2) K θmin = 4.5º
φ and ω scans h = −12→12
Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2007) k = −15→17
Tmin = 0.874, Tmax = 0.974 l = −22→22
19776 measured reflections