| Oxford Diffraction Gemini R CCD diffractometer | 8636 independent reflections |
| Radiation source: fine-focus sealed tube | 4667 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.027 |
| Detector resolution: 10.5081 pixels mm-1 | θmax = 32.5º |
| T = 296(2) K | θmin = 4.5º |
| φ and ω scans | h = −12→12 |
| Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2007) | k = −15→17 |
| Tmin = 0.874, Tmax = 0.974 | l = −22→22 |
| 19776 measured reflections |