| Refinement on F2 | Secondary atom site location: difference Fourier map |
| Least-squares matrix: full | Hydrogen site location: inferred from neighbouring sites |
| R[F2 > 2σ(F2)] = 0.047 | H-atom parameters constrained |
| wR(F2) = 0.127 | w = 1/[σ2(Fo2) + (0.0653P)2] where P = (Fo2 + 2Fc2)/3 |
| S = 0.97 | (Δ/σ)max = 0.001 |
| 8636 reflections | Δρmax = 0.31 e Å−3 |
| 363 parameters | Δρmin = −0.23 e Å−3 |
| Primary atom site location: structure-invariant direct methods | Extinction correction: none |