Nonius Kappa CCD diffractometer | 3765 independent reflections |
Radiation source: fine-focus sealed tube | 3186 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.069 |
Detector resolution: 9 pixels mm-1 | θmax = 28.7º |
T = 120(2) K | θmin = 2.8º |
φ and ω scans | h = −11→11 |
Absorption correction: multi-scan(SADABS; Sheldrick, 2003) | k = −11→11 |
Tmin = 0.720, Tmax = 0.888 | l = −16→16 |
11529 measured reflections |