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. 2007 Dec 6;64(Pt 1):m37–m38. doi: 10.1107/S1600536807058928
Nonius Kappa CCD diffractometer 3765 independent reflections
Radiation source: fine-focus sealed tube 3186 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.069
Detector resolution: 9 pixels mm-1 θmax = 28.7º
T = 120(2) K θmin = 2.8º
φ and ω scans h = −11→11
Absorption correction: multi-scan(SADABS; Sheldrick, 2003) k = −11→11
Tmin = 0.720, Tmax = 0.888 l = −16→16
11529 measured reflections