| Bruker X8 KappaCCD APEXII diffractometer | 3736 independent reflections |
| Radiation source: fine-focus sealed tube | 2523 reflections with I > 2σ(I) |
| graphite | Rint = 0.061 |
| ω/φ scans | θmax = 26.0°, θmin = 3.8° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1998) | h = −11→9 |
| Tmin = 0.982, Tmax = 0.984 | k = −22→23 |
| 19608 measured reflections | l = −13→13 |
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