| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.038 | w = 1/[σ2(Fo2) + (0.0502P)2 + 0.2861P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.100 | (Δ/σ)max < 0.001 |
| S = 1.06 | Δρmax = 0.22 e Å−3 |
| 2860 reflections | Δρmin = −0.25 e Å−3 |
| 235 parameters | Extinction correction: SHELXL, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| Primary atom site location: structure-invariant direct methods | Extinction coefficient: 0.013 (3) |
| Secondary atom site location: difference Fourier map |