Bruker SMART APEX CCD area-detector diffractometer | 2611 independent reflections |
Radiation source: fine-focus sealed tube | 1053 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.129 |
T = 293(2) K | θmax = 25.0º |
0.3° wide ω scans | θmin = 2.3º |
Absorption correction: multi-scan(SADABS; Bruker, 2000) | h = −24→18 |
Tmin = 0.820, Tmax = 0.852 | k = −11→11 |
7479 measured reflections | l = −20→20 |