Enraf–Nonius CAD-4 diffractometer | Rint = 0.017 |
Radiation source: fine-focus sealed tube | θmax = 27.0º |
Monochromator: graphite | θmin = 1.7º |
T = 293(2) K | h = 0→8 |
ω scans | k = 0→28 |
Absorption correction: none | l = −8→8 |
2964 measured reflections | 3 standard reflections |
2764 independent reflections | every 100 reflections |
2022 reflections with I > 2σ(I) | intensity decay: none |