Bruker APEX CCD area-detector diffractometer | 4424 independent reflections |
Radiation source: fine-focus sealed tube | 2623 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.109 |
T = 293(2) K | θmax = 25.3º |
ω scans | θmin = 1.6º |
Absorption correction: empirical (using intensity measurements)(SADABS; Sheldrick, 1996) | h = −10→10 |
Tmin = 0.970, Tmax = 0.982 | k = −24→30 |
12521 measured reflections | l = −13→13 |